Fabrication and the effect of Sb2O3 nanoparticles on Bi-2223 superconductor

Abstract

In this paper Sb2O3 nanoparticles are synthesized by solution method. The effect of these nanoparticles on the Bi-2223 superconductor properties has been investigated. The critical temperature, critical current density and activation energy were measured by the standard four-probe method. Magnetic properties of the samples were measured by using the AC magnetic susceptibility. The microstructure and morphology of samples have been studied by X-ray diffraction, scanning electron microscope and energy dispersive X-ray. The results of X-ray diffraction patterns show that the low amount of Sb2O3 and long annealing time enhance the fraction of Bi -2223 phase. Also the results show that the Sb2O3 nanoparticles do not change the phases and critical temperature of Bi-2223 superconductor, but by increasing the amount of Sb2O3 nanoparticles, the critical current density and the activation energy of the samples increase.

Keywords


[1] Turker M., "Effect of production parameters on the structure andmorphology of Ag nanopowders produced by inert gas condensation", Material Science and Engineering A 367 (2004) 74.

[2] Murry Hill, "Nanotechnology", Grerory. Timp Bell babaratories, (1999) part 1&2.

[3] Zeng D. W., Xie C. S., Zhu B. L. and Sang W. L., "Characteristicsof Sb2O3 nanoparticles synthesized from antimony by vapor condensation method", Mater. Lett. 58 (2004312) 312.

[4] Cui Z., Zhang Z., Hao C., Dong L., Meng Z. and Yu L., "Structures and properties of nano-particles prepared by hydrogen arc plasma method", Thin Solid Films 318 (1998) 76.

[5] Ye C., Wang G., Kong M., Zhang L., "Controlled synthesis of Sb2O3 nanoparticles nanowires and nanoribbons", Journal Nanometerials, 2006 (2006) 1.

[6] Bocanegra- Diaz A., Mohallem N. S., Sinisterra R. D., "Preparation of a ferrofluid using cyclodextrin and magnetite", J. Braz. Chem. Soc. 14 (2003) 936.

[7] Jasiolek G., Gorecka J., Majewskit G., Yuan S., Jin S., Lianng R., "X-ray characterization of Bi-Pb-Sr-Ca-Cu-O ceramic", Supercond. Sci. Technol. 3 (1990) 194.

[8] Vlasse M., Golben J., Mitchell T., "Process optimization for the Pb and Sb substituted Bi- based 2223 bulk ceramic superconductors", Supercond. Sci. Technol. 5 (1992) 236.

[9] Chu C. W., Bechtold J., Gao L., Hor P. H., Xue Y. Y., "Superconductivity up to 114K in the Bi-Al-Ca-Sr-Cu-O compound system without rare-earth elements", Phys. Rev. Lett. 60 (1988) 941.

[10] Dou S. X., Liu A. J., Bourdillon M., Kviz N. X., Sorrell C. C., "Stability of superconducting phases in Bi-Sr-Ca-Cu-O and the role of Pb doping", Phys. Rev. B 40 (1989) 5266.

[11] Popov A. G., Dovgopo V. P. l, Olevsky F. M., Melnikov V. S., Pan V. M., "The superconductivity of the Sb-doped Bi-Pb-Sr-Ca-Cu-O Compounds", Supercond. Sci. Technol .5 (1992) 654.

[12] Agnihotry S. A., Ghosai P., Nagpai K. C., Chandra S., "Enhancement of Tcon appearance of a new phase and faster kinetics in Pb+Sb doped Bi2Sr2Ca2Cu3Oy", Supercond. Sci. Technol. 4 (1991) 7.

[13] Sarkar B., Reddy Y.S., Sharma R. G., "Effect of Sb doping on critical current density in Bi (Pb)-Sr-Ca-Cu-O high Tc superconductors" , Physica C 219 (1994) 26.

[14] Zargar Shoushtari M., Bahrami A., Farbod M., "The effect of silver doping on the critical current density of Bi-Pb-Sr-Ca-Cu-O ceramic superconductor". Phys. Stat. Sol. (c), 3 (2006) 2994.

[15] Zargar Shoushtari M., Mousavi Ghahfarokhi S. E., Farbod M., "The Effect of Cd Doping on Bi-Based Superconductor". Journal of Applied Sciences 8, 14 (2008) 2613.

[16] مدنی، حسن ، "اصول پی‌جویی، اکتشاف و ارزیابی ذخائر معدنی"، چاپ دوم 1368 صفحه 149.

[17] Chikazami S., Charap S. H., "Physics of Magnetism" Jhon wiley, Newyork (1964).

[18] Kameli P., Salamati H., Eslami M., "The effect of sintering temperature on the intergranular properties of Bi-2223 superconductora", Solid State Communications 137 (2006) 30.

[19] موسوی قهفرخی سید ابراهیم، زرگر شوشتری مرتضی، فربد منصور، همایش بلورشناسی وکانی‌شناسی ایران، مشهد، بهمن‌ماه 1386

[20] Zargar Shoushtari M., Kashian M. R., Yazdani H., "Study on the Properties of Bi1.6Pb0.4Sr2Ca2Cu2+xOy". Physica B 321 (2002) 305.

[21] Han G. C., "Voltage-current characteristics in C- axis-oriented Bi1.8Pb0.4Sr2Ca2Cu3O/Ag tapes", J. Phys. Condens. Matter 7 (1995) 8175.

[22] Sun J. Z., Eom C. B., Lairson B., Bravman J. C. and Gceballe T. H., "Magnetic relaxation current-voltage characteris and possible dissipation mechanisms for high-Tc-superconducting thin films of Y-Ba-Cu-O", Phys. Rew B 43 (1991) 3002.

[23] Mousavi Ghahfarokhi S. E., Zargar Shoushtari M., Farbod M., "Study of Bi1.65-xPb0.35SbxSr2 Ca2Cu3Oy Superconductor". Journal of Applied Sciences 9, 4 (2009) 783.

[24] Liu R. Y., Naite H., Okuda M. K., Nakahigashi Y. Takingawa, T. Mastsushita, K. K. Kurosawa, "Effects of Sb and Pb doping on the high Tc phase formation in Bi-Sr-Ca-Cu-O superconductors", Supercond. Sci. Technol. 5 (1992) 482.

[25] Qidwai A. A., Humayan M., Zia-ul-Haque S. M., Dabir A. and Saghir A., "Preparation and high Tc measurements of the Bi1.6-Pbx-Sby-Sr2-Ca2Cu3O superconducting system with x = 0.4, 0.3, 0.1 and

y = 0, 0.1, 0.3", Supercond. Sci. Technol. 5 (1992) 602.