The growth of alkali halide cesium iodide single crystal in five zone furnace by Bridgman method

Document Type : Original Article

Abstract

In this research, the vertical Bridgman method has used to perform the single crystal growth of cesium iodide alkali halide. To this purpose, a vertical cylindrical furnace equipped with electric elements with five different thermal regions has been designed and constructed. The temperature gradient of the furnace can be controlled up to 1000○C with 0.1○C accuracy. Several cesium iodide sample crystals has been grown with this furnace and then the X-ray diffraction characterizations have been undertaken. The photoluminescence spectrum and the hardness properties of the crystals samples have been studied as well as the measurements of etch-pits of single crystals. Since the pure cesium iodide exhibits scintillation properties, the gamma-ray spectroscopy has also been undertaken.  

Keywords


  1. [1] Daisuke Totsuka, Takayuki Yanagida, Yutaka Fujimoto, "Growth and scintillation properties of pure CsI crystal grown by micro-pulling-down method", Optical. Math. 34(2012) 1087-1091. [DOI:10.1016/j.optmat.2012.01.003]
  2. [1] Daisuke Totsuka, Takayuki Yanagida, Yutaka Fujimoto, "Growth and scintillation properties of pure CsI crystal grown by micro-pulling-down method", Optical. Math. 34(2012) 1087-1091. [DOI:10.1016/j.optmat.2012.01.003]
  3. [2] Gridin S., Belsky A., Moszynski M., "Scintillation properties CsI:In single crystals", Nucl. Instr. And Meth. A 761(2014) 13-18. [DOI:10.1016/j.nima.2014.05.111]
  4. [2] Gridin S., Belsky A., Moszynski M., "Scintillation properties CsI:In single crystals", Nucl. Instr. And Meth. A 761(2014) 13-18. [DOI:10.1016/j.nima.2014.05.111]
  5. [3] Marvin J.weber., "Inorganic scintillators: today and tomorrow", Journal of Luminescence 100 (2002) 35–45 [DOI:10.1016/S0022-2313(02)00423-4]
  6. [3] Marvin J.weber., "Inorganic scintillators: today and tomorrow", Journal of Luminescence 100 (2002) 35–45 [DOI:10.1016/S0022-2313(02)00423-4]
  7. [4] Guohao Ren., Xiaofeng Chen., Sheng Lu., "Non-uniformity of light output in large-sized CsI(Tl) crystals grown by non-vacuum Bridgman method", Nuclear Instruments and Methods in Physics Research A 564 (2006) 364–369 [DOI:10.1016/j.nima.2006.05.081]
  8. [4] Guohao Ren., Xiaofeng Chen., Sheng Lu., "Non-uniformity of light output in large-sized CsI(Tl) crystals grown by non-vacuum Bridgman method", Nuclear Instruments and Methods in Physics Research A 564 (2006) 364–369 [DOI:10.1016/j.nima.2006.05.081]
  9. [5] Balamurugan N., Arulchakkaravarthi A., Selvakumar S., Lenin S., Rakesh Kumar S., Muralithar K., Sivaji P., Ramasamy "Growth and characterization of undoped and thallium doped cesium iodide single crystals", J. Crys. Grow. 286 (2006) 294-299. [DOI:10.1016/j.jcrysgro.2005.08.057]
  10. [5] Balamurugan N., Arulchakkaravarthi A., Selvakumar S., Lenin S., Rakesh Kumar S., Muralithar K., Sivaji P., Ramasamy "Growth and characterization of undoped and thallium doped cesium iodide single crystals", J. Crys. Grow. 286 (2006) 294-299. [DOI:10.1016/j.jcrysgro.2005.08.057]
  11. [6] Zaslavsky B.G., "Automated pulling of large-diameter alkali halide scintillation single crystals from the melt", Journal of Crystal Growth 200 (1999) 476-482 [DOI:10.1016/S0022-0248(98)01404-3]
  12. [6] Zaslavsky B.G., "Automated pulling of large-diameter alkali halide scintillation single crystals from the melt", Journal of Crystal Growth 200 (1999) 476-482 [DOI:10.1016/S0022-0248(98)01404-3]
  13. [7] Moszynski M., "Inorganic scintillation detectors in g-ray spectrometry", Nuclear Instruments and Methods in Physics Research A 505 (2003) 101–110 [DOI:10.1016/S0168-9002(03)01030-1]
  14. [7] Moszynski M., "Inorganic scintillation detectors in g-ray spectrometry", Nuclear Instruments and Methods in Physics Research A 505 (2003) 101–110 [DOI:10.1016/S0168-9002(03)01030-1]
  15. [8] Mori Y., Kayal A.H., Jaccard C., "A SEARCH FOR Na ATOM IN Csl:Na CRYSTAL", Solid State Communications, 4 (l)(1982)69-74.. [DOI:10.1016/0038-1098(82)90251-4]
  16. [8] Mori Y., Kayal A.H., Jaccard C., "A SEARCH FOR Na ATOM IN Csl:Na CRYSTAL", Solid State Communications, 4 (l)(1982)69-74.. [DOI:10.1016/0038-1098(82)90251-4]
  17. [9] BRINCKMANN S., "Csl(Na) SCINTILLATION CRYSTALS". Phys. Lett. 15 (1965) 305. [DOI:10.1016/0031-9163(65)91262-X]
  18. [9] BRINCKMANN S., "Csl(Na) SCINTILLATION CRYSTALS". Phys. Lett. 15 (1965) 305. [DOI:10.1016/0031-9163(65)91262-X]
  19. [10] Maria da Conceicao C. Pereira, Margarida Mizue Hamada, "Luminescence and scintillation characteristics in the CsI:Br crystal on Br concentrations", Nucl. Instr. And Meth. A 537 (2005) 189-192. [DOI:10.1016/j.nima.2004.08.005]
  20. [10] Maria da Conceicao C. Pereira, Margarida Mizue Hamada, "Luminescence and scintillation characteristics in the CsI:Br crystal on Br concentrations", Nucl. Instr. And Meth. A 537 (2005) 189-192. [DOI:10.1016/j.nima.2004.08.005]