تهیه و شناسایی کمپلکس پروپیون آمید - اکسالیک اسید به روش پراش سنجی پودری پرتو x

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دانشگاه اصفهان

چکیده

کمپلکس C2H5CONH2(COOH)2 از اکسالیک اسید، (COOH)2 و پروپیون آمید C2H5CONH2 ب نسبت مولی 1:1 در شرایط ویژه ای تهیه، و به روش پراش سنجی پودری پرتو X با طول موج ...

کلیدواژه‌ها


عنوان مقاله [English]

Synthesis and Powder Diffraction Analysis of Propionamide Oxalic Acid Complex.

چکیده [English]

A propionamidc oxalic acid complex was prepared
flOm propionamidc and oxalic aCid . It was a bright and
hygroscopic compound with vcry low hardness and was
accompanied with deformation in air at room temperature. lis
X - ray powder diffraction data were collected by a computer
diffractometer and was analyLCd by profile analysis tcchniqucs.
The compound was crystallized in triclinic system with
space group P T. Lallioo pammetcr:i were 35 follows:
a = 6.334(4)A b = IO.486(6)A < = 7.225(4) A
a = 85.55(3)' fJ = 82.20(1)" ,Y = 80.03(2)"
V = 466.6(5)A D, = 1.16 g

کلیدواژه‌ها [English]

  • Propionamide Oxalic Acid Complex
  • SyntiJesis
  • Crystal SrmclUre